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Reproducibility Note · N°01

Human acetylcholinesterase

PDB 4EY7 Alzheimer's disease Workflow-sensitive self-docking 0.27 Å

The claim

Published docking studies on human acetylcholinesterase (AChE, PDB 4EY7) report dietary flavonoids as inhibitors with AutoDock Vina scores spanning roughly −8.6 to −12.6 kcal/mol. A few values stand out as unusually strong, notably rutin at −12.6 and epicatechin gallate at −12.2 kcal/mol.

The re-execution

We first confirmed the engine recovers the co-crystallised ligand (donepezil) in 4EY7 by self-docking: RMSD 0.27 Å, well below the 2 Å threshold. Twenty-two public phytochemicals were then re-executed with three fixed seeds (11, 29, 53), AutoDock Vina at exhaustiveness 64, GNINA deep-learning rescoring, PLIP interactions and a consensus score (ADS, 0–100). Seed-to-seed noise was low (median SD 0.03 kcal/mol).

This is a proof-of-concept pilot: only the literature anchor values supplied in our study brief are compared, and no published figure was invented.

Multi-angle reading

Compound Reported Vina GNINA ADS ± 2 Interactions
Luteolin · CID 5280445 -10.36 0.42 82.6 11 H-bonds, 6 hydrophobic
Quercetin · CID 5280343 -10.18 0.26 77.9 12 H-bonds, 7 hydrophobic
Apigenin · CID 5280443 -10.19 0.32 79.6 7 H-bonds, 7 hydrophobic
Kaempferol · CID 5280863 -9.79 0.34 80.1 10 H-bonds, 7 hydrophobic
Rutin · CID 5280805 -12.6 Vina (lit.) -10.13 0.44 33.1 MW 610, Lipinski-fail, poor ligand efficiency
Epicatechin gallate · CID 107905 -12.2 Vina (lit.) -9.15 0.23 33.2 GNINA-contradicted; −12.2 only in a tight gorge box
Donepezil (reference) · CID 3152 -11.33 0.69 76.2 Co-crystal reference; self-docking 0.27 Å

Vina in kcal/mol (lower = better) · GNINA CNN score 0–1 (higher) · ADS consensus /100 (higher). "± 2" = Vina deviation from the reported value within the 2.0 kcal/mol tolerance.

3D exploration

Fullscreen →

Interactive companion: the target pocket in 3D, the real docking poses, and the whole pipeline (Vina, GNINA, drug-likeness, ML/DTI, consensus) explained step by step.

The finding

The mid-range flavonoid scores reproduce cleanly and stably (−9.8 to −10.4 kcal/mol). The eye-catching −12 values do not. Rutin's reported −12.6 is not reachable in any box tested here (best −10.1); epicatechin gallate's −12.2 appears only when the search box is tightly centred on the catalytic gorge: a whole-protein search gives −9.15, a 3 kcal/mol swing larger than the entire seed-noise budget.

Read by Vina alone, rutin (−10.1) and epicatechin gallate would tie the genuine flavonoids. The multi-angle consensus tells a different story: it demotes both to ≈ 33 / 100 (vs 76–83 for luteolin, kaempferol, apigenin) because of poor ligand efficiency, a Lipinski failure for rutin (MW 610), and a GNINA pose-quality contradiction for epicatechin gallate. The discrepancies track with under-specified search boxes, not with any error attributable to the authors.

Methods lesson

A single, very low Vina ΔG on a large or oversized phytochemical is more often an artefact of the search box or protocol than a real affinity. Reporting the box centre and size, plus a random seed, and reading a score alongside ligand efficiency and a second engine, is what turns a docking number into a re-executable, trustworthy claim.

Source

Proof-of-concept pilot. Only literature anchor values supplied in our study brief are compared here; full source-paper verification is part of the planned scale-up. No published value was invented.